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23. Patel, D. ; Itakura, K . Science, 1982, 216, 581. ; Weber, T. ; Runnels, J. H. NMR OF SOLID POLYMERS 2 An Introduction to NMR Spectroscopy of Solid Samples DANIEL J. O'DONNELL Phillips Petroleum Company, Bartlesville, OK 74004 Complex solid sample NMR techniques used in other chapters of this text are discussed. These techniques are presented using conceptual arguments, rather than mathematical equations, so that those unfamiliar with NMR spectroscopy might get a quick grasp of the nature of the experiment.
Couplings, 31 while retaining ^-H- F i n a l l y , i t s h o u l d be p o i n t e d o u t t h a t t h e above d i s c u s s i o n s are vast over-simplifications which are (hopefully) conceptually easy t o grasp. unfortunately, they are not theoretically satisfying. A d d i t i o n a l reading i s urged t o pro v i d e a more i n d e p t h understanding(1-5). Cross P o l a r i z a t i o n C l a s s i c a l l y , t h e n e t magnetization, M , o f a s p i n system r e s u l t s f r o m t h e sum o f t h e i n d i v i d u a l s p i n s w h i c h p r e c e s s a b o u t t h e applied field, H (see F i g .
G. J. Am. Chem. , 1957, 79, 3289. 4. ; Wishnia, A. Y. Acad. , 1958, 70 870. 5. Odajima, A. J. Phys. Soc. , 1959, 14, 777. 6. Bovey, F. ; Tiers, G. V. ; Filipovich, G. J. Polym. , 1959, 38, 73. 7. Bovey, F. ; Tiers, G. V. D. J. , 1960, 44, 173. 8. , 1960, 48, 241. 9. Chen, Η. Y. Anal. , 1962, 34, 1134, 1793. 10. Golub, Μ. ; Fuqua, S. ; Bhacca, N. S. J. Am. Chem. , 1962, 84, 4981. 11. Wilson III, C. W. J. Polym. , 1963, Part A1, 1305. 12. Wilson III, C. , E. R. J. Polym. , 1965, Part C8, 97. 13. Bovey, F.